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The effect of surface treatments of glass capillaries on column performance

Research paper by M. H. J. van Rijswick, K. Tesařík

Indexed on: 01 Mar '74Published on: 01 Mar '74Published in: Chromatographia



Abstract

The effects of etching and/or silylation of glass capillaries on column efficiency were studied. Coated with apolar OV-101, only columns subjected to the combined treatment showed an increase of about 50% in the number of effective plates. Surface hydroxylation, prior to silylation, gave a small additional improvement for this stationary phase.